Polycrystalline solids under nonhydrostatic compression: Determination of strength from x-ray diffraction data

Singh, AK (2014) Polycrystalline solids under nonhydrostatic compression: Determination of strength from x-ray diffraction data. Journal of Physics: Conference Series, 500.

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Abstract

A polycrystalline sample compressed in a diamond anvil cell (DAC) without any pressure transmitting medium develops a stress state at the centre of the sample that is axially symmetric about the load axis. The axial stress component is larger than the radial component and the difference t between the two is taken as a measure of the compressive strength of the sample material at a confining pressure that equals the mean normal stress. A proper analysis of the diffraction data yields t. The data taken with the radial diffraction geometry, wherein the incident x-ray beam is perpendicular to the load axis of the DAC, give reliable estimates of strength. The diffraction data obtained with the conventional geometry, wherein the incident x-ray beam passes parallel to the DAC axis, provide reasonable estimates of strength. However, even in this case, reliable strength data can be obtained by combining the measured pressure-volume data under nonhydrostatic compression and the hydrostat derived from an independent source. The determination of strength from high pressure diffraction data is discussed.

Item Type:	Article
Subjects:	CHEMISTRY AND MATERIALS > Chemistry and Materials (General)
Depositing User:	Mr. BS Shivaram
Date Deposited:	19 Dec 2014 08:19
Last Modified:	19 Dec 2014 08:19
URI:	http://nal-ir.nal.res.in/id/eprint/12056

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