Failure of reformer tube of an ammonia plant

Bhaumik, SK and Rangaraju, R and Parameswara, MA and Bhaskaran, TA and Venkataswamy, MA and Raghuram, AC and Krishnan, RV (2002) Failure of reformer tube of an ammonia plant. Engineering Failure Analysis, 9 (5). pp. 553-561.

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Abstract

The present article describes the failure of a primary reformer tube in an ammonia plant. The failure took place at the stub end of the reformer tube where a SS 321 flange was joined to a HK 40 catalyst tube by welding. Detailed metallurgical examinations indicated that the failure was due to stress corrosion cracking. Both longitudinal and transverse cracks were observed at the region of fracture. The cracks originated at the interface of the weld and HAZ at the inner surface and progressed to the outside of the tube in the transverse (thickness) direction. Microstructural study revealed chromium carbides precipitation at the grain boundaries in the heat affected zones on either sides of the weld. The results clearly indicated that the steel had undergone sensitisation which subsequently led to failure of the reformer tube by stress corrosion cracking. xA9; 2002 Published by Elsevier Science Ltd.

Item Type: Journal Article
Uncontrolled Keywords: Chemical-plant failures; Sensitisation; Stress corrosion cracking; Weld decay; Welded fabrications; Ammonia; Grain boundaries; Metallurgy; Stress corrosion cracking; Tubes (components); Welding; Reformer tubes; Industrial plants; chemical plant; fabrication; failure analysis; stress corrosion cracking; welded joint;
Subjects: CHEMISTRY AND MATERIALS > Chemistry and Materials (General)
Division/Department: Materials Science Division, Other, Materials Science Division, Materials Science Division, Materials Science Division, Other, Materials Science Division
Depositing User: MS Jayashree S
Date Deposited: 07 Jan 2005
Last Modified: 24 May 2010 09:38
URI: http://nal-ir.nal.res.in/id/eprint/81

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